It’s a bit puzzling initially as both the SHYMAN (Sustainable Hydrothermal Manufacturing of Nanomaterials) project and Promethean Particles are claiming to be the world’s biggest nanomaterials production facility. In a battle of press release titles (one from CORDIS and one from the University of Nottingham) it becomes clear after reading both that the SHYMAN project is the name for a European Commission 7th Framework Programme funded project and Promethean Particles, located at the University of Nottingham (UK), is a spinoff from that project. So, both claims are true, although confusing at first glance.
An Aug. 1, 2016 news item on Nanowerk breaks the news about the ‘SHYMAN project’s’ production facility (Note: A link has been removed),
The European SHYMAN project aims to establish continuous hydrothermal synthesis as the most flexible and sustainable process to create nanomaterials at industrial scale. After demonstrating this potential in the lab, the project has now announced the opening of its first facility in Nottingham.
An (Aug. 1, 2016?) CORDIS press release, which originated the news item,
‘This new facility opens up a significant amount of new opportunities for us,’ says Professor Ed Lester, Technical Coordinator of Promethean Particles. This spin-out of the University of Nottingham is in charge of operating the new plant, which is expected to produce over 1 000 tonnes of nanomaterials every year. The production cost is lower than that of other facilities and the chosen production method – continuous hydrothermal synthesis – is expected to impact even markets for which sale prices had so far been an obstacle.
‘We have already had a lot of interest from companies in a diverse range of sectors. From healthcare, where nano-particles can be used in coatings on medical devices, to enhanced fabrics, where nano-materials can add strength and flexibility to textiles, and in printed electronics, as we are able to print materials such as copper,’ Prof. Lester continues. Solvay, Fiat, PPG and Repsol are among the major companies already set to benefit from the plant’s products.
To reach these impressive levels of production, the plant notably relies on high pressure triplex plunger pumps manufactured by Cat Pumps. These pumps have helped the 18-strong consortium to overcome engineering issues related to the mixing of the heated fluid and the aqueous metal salt flow, by creating the continuous pressure and fluid flow necessary to achieve continuous production.
Another enabling technology is the Nozzle Reactor, a customised design that uses buoyancy-induced eddies to produce an ‘ideal’ mixing scenario in a pipe-in-pip concentric configuration in which the internal pipe has an open-ended nozzle. This technology allows Promethean Particles to dramatically improve reproducibility and reliability whilst controlling particles properties such as size, composition and shape.
Betting on hydrothermal synthesis
Started in 2012, SHYMAN built upon the observation that hydrothermal synthesis had numerous advantages compared to alternatives: it doesn’t resort to noxious chemicals, uses relatively simple chemistry relying on cheap precursors, allows straightforward downstream processing, can avoid agglomeration and allows for narrow and well-controlled size and shape distribution.
The optimisation of hydrothermal synthesis has been a key objective of the University of Nottingham for the past 14 years, and SHYMAN is the pinnacle: the project began with the development of bench scale reactors, followed by a 30-times-larger pilot scale reactor. The reactor at the heart of the new production plant is 80 times larger than the latter and features four Cat Pumps Model 3801 high pressure triplex plunger pumps.
‘These are very exciting times for Promethean Particles,’ said Dr Susan Huxtable, Director of Intellectual Property and Commercialisation at the University of Nottingham. ‘The new facility opens up a myriad of opportunities for them to sell their services into new markets right across the world. It is a great example of how many of the technologies developed by academics here at the University of Nottingham have the potential to benefit both industry and society.’
The July 12, 2016 University of Nottingham press release, while covering much of the same ground, offers some additional detail,
The plant [Promethean Particles] was developed as part of a pan-European nano-materials research programme, known as SHYMAN (Sustainable Hydrothermal Manufacturing of Nanomaterials). The project, which had a total value of €9.7 million Euros, included partner universities and businesses from 12 European countries.
The outcome of the project was the creation of the largest multi-material nano-particle plant in the world, based in Nottingham. The plant is now operated by Promethean, and it is able to operate at supercritical conditions, producing up to 200 kg of nano-particles per hour.